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RESEARCH PRODUCTS NMR Solvent Data Chart

LThe 1H spectra of the residual protons and 13C spectrawere obtained on a Varian Gemini 200 spectrometerat 295 K. The NMR solvents used to acquire thesespectra contain a maximum of and TMS(v/v) respectively. Since deuterium has a spin of 1,triplets arising from coupling to deuterium have theintensity ratio of 1:1:1. m denotes a broad peak withsome fine structures. It should be noted that chemicalshifts can be dependent on Solvent , concentrationand values only, may vary with pH, concen-tration and and boiling points are those of the corre-sponding unlabeled compound (except for D2O).These temperature limits can be used as a guide todetermine the useful liquid range of the gathered from the Merck Index Fourteenth Edition.

12 / Deuterium Oxide / N,N-Dimethylformamide-d 7 / Dimethyl Sulfoxide-d 6 / 1,4-Dioxane-d 8 (p-Dioxane) / Ethanol-d 6 / Methanol-d 4 / Methylene Chloride-d 2 / Pyridine-d 5 / 1,1,2,2 Tetrachloroethane-d 2 / Toluene-d 8 / Trifluoroacetic Acid-d / 2,2,2-Trifluoroethanol-d 3 Store at room temperature away from light and moisture.

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  Dimethylformamide, N dimethylformamide

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