(2) Proton-decoupled C NMR Spectra
obtaining 13C NMR spectra is called a proton-decoupled (or broad-band decoupled) method. (2) Proton-decoupled 13C NMR Spectra As in the case of 1H NMR, 13C NMR spectra are obtained typically in CDCl 3 with tetramethylsilane (TMS) as internal reference, i.e., δ = 0 ppm for TMS methyl carbons. Most of the 13C NMR chemical
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