Agilent InfinityLab LC Series

1 VialsamplersAgilent InfinityLab LC SeriesUser ManualAgilent InfinityLab LC Series Vialsamplers User ManualAgilent InfinityLab LC Series Vialsamplers User ManualNoticesDocument InformationDocument No: SD-29000242 Rev. E Part No: G7129-90010 Rev. E EDITION 04/2020 Copyright Agilent Technologies, Inc. 2015-2020No part of this manual may be repro-duced in any form or by any means (including electronic storage and retrieval or translation into a foreign language) without prior agreement and written con-sent from Agilent Technologies, Inc. as governed by United States and interna-tional copyright Technologies Hewlett-Packard-Strasse 8 76337 WaldbronnWarrantyThe material contained in this document is provided as is, and is subject to being changed, without notice, in future edi-tions.

2 Further, to the maximum extent permitted by applicable law, Agilent dis-claims all warranties, either express or implied, with regard to this manual and any information contained herein, includ-ing but not limited to the implied warran-ties of merchantability and fitness for a particular purpose. Agilent shall not be lia-ble for errors or for incidental or conse-quential damages in connection with the furnishing, use, or performance of this document or of any information con-tained herein. Should Agilent and the user have a separate written agreement with warranty terms covering the material in this document that conflict with these terms, the warranty terms in the separate agreement shall Licenses The hardware and/or software described in this document are furnished under a license and may be used or copied only in accordance with the terms of such Rights Government Restricted Rights.

3 Soft-ware and technical data rights granted to the federal government include only those rights customarily provided to end user customers. Agilent provides this customary commercial license in Soft-ware and technical data pursuant to FAR (Technical Data) and (Computer Software) and, for the Depart-ment of Defense, DFARS (Technical Data - Commercial Items) and DFARS (Rights in Commer-cial Computer Software or Computer Software Documentation).Safety NoticesCAUTIONA CAUTION notice denotes a hazard. It calls attention to an operating procedure, practice, or the like that, if not correctly per-formed or adhered to, could result in damage to the product or loss of important data.

4 Do not proceed beyond a CAUTION notice until the indicated conditions are fully understood and met. WARNINGA WARNING notice denotes a hazard. It calls attention to an operating procedure, practice, or the like that, if not correctly per-formed or adhered to, could result in personal injury or death. Do not proceed beyond a WARN-ING notice until the indicated conditions are fully understood and InfinityLab LC Series Vialsamplers User Manual3 In This Book:This manual covers the following modules: Agilent 1260 infinity II Vialsampler (G7129A) Agilent 1290 infinity II Vialsampler (G7129B) Agilent 1260 infinity II Vialsampler (G7129C)

5 1 Introduction This chapter gives an introduction to the module and instrument Requirements and Specifications This chapter provides information on environmental requirements, physical and performance the Module This chapter provides information on how to use the the Module This chapter explains the operational parameters of the Performance This chapter provides information on how to optimize the and Diagnostics This chapter gives an overview of the maintenance, troubleshooting, and diagnostic features available for the Agilent InfinityLab Series Information This chapter describes the meaning of error messages.

6 And provides information on probable causes and suggested actions how to recover from error InfinityLab LC Series Vialsamplers User Manual4 8 Maintenance This chapter describes the maintenance of the and Materials for Maintenance This chapter provides information on parts for Cables This chapter provides information on cables used with the Agilent 1200 infinity Series Information This chapter describes the detector in more detail on hardware and Configuration This chapter provides information on connecting the module to the Agilent ChemStation This chapter provides additional information on safety, legal and InfinityLab LC Series Vialsamplers User Manual5 Contents1 Introduction 9 Product Description (G7129A) 10 Features (G7129A) 11 Product Description (G7129B) 12 Features (G7129B) 13 Product Description (G7129C) 14 Features (G7129C)

7 15 Overview of the Module 16 Operating Principle 18 Leak and Waste Handling 272 Site Requirements and Specifications 33 Site Requirements 34 Physical Specifications 38 Performance Specifications 39 Specifications of the Sample Cooler 47 Specifications of the Sample Thermostat 49 Specifications of the Integrated Column Compartment 513 Using the Module 53 Magnets 55 Turn on/off 56 Status Indicators 58 Vial Drawers and Trays 59 Choice of Vials and Caps 70 Install the Optional Integrated Column Compartment 74 Using the Optional Integrated Column Compartment 96 Install the Optional Sample Cooler/Sample Thermostat 116 Using the Optional Sample Cooler/Sample Thermostat 123 Transporting the Sampler 132 Agilent Local Control Modules 137 Agilent InfinityLab LC Series Vialsamplers User Manual6 4 Preparing the Module 139 Leak and Waste Handling 140 Preparing the Module 141 Solvent Information 142 Capillary Color Coding Guide 149 Installing Capillaries 150 Flow Connections to the Vialsampler 152 Setting up the Vialsampler 1545 Optimizing Performance 166

8 Optimization for Lowest Carryover 167 Fast Injection Cycle and Low Delay Volume 171 Precise Injection Volume 173 Choice of Rotor Seal 1756 Troubleshooting and Diagnostics 176 Status Indicators 177 Overview of Tests and Tools 178 Maintenance and Troubleshooting Tools 179 Diagnostic Tests 187 Agilent Lab Advisor Software 1897 Error Information 190 What are Error Messages 192 General Error Messages 193 Vialsampler Error Messages 201 Sample Cooler/Sample Thermostat Error Messages 213 Integrated Column Compartment (ICC) Heater Error Messages 219 Agilent InfinityLab LC Series Vialsamplers User Manual7 8 Maintenance 222 Introduction to Maintenance 223 Warnings and Cautions 224 Overview of Maintenance 226 Cleaning the Module 227 Remove and Install Doors 228 Exchange the Needle Assembly 229 Exchange the Needle Seat Assembly 235 Exchange the Sample Loop Assembly 241 Exchange the Rotor Seal 245 Exchange the Metering Seal and Piston 250 Replace the Analytical Heads 255 Exchange the Gripper Arm 258 Replace the Peristaltic Pump Cartridge 261 Exchange

9 The Wash Port Assembly 263 Replace the Module Firmware 269 Replace the Sample Cooler/Sample Thermostat 2709 Parts and Materials for Maintenance 275 Standard Parts For Maintenance 276 Accessory Kits 279 Vial Drawers and Trays 283 Multidraw Kits 286 Sample Thermostat Upgrade 287 Integrated Column Compartment 288 Column ID Upgrade Kit 289 Parts for 900 L Injection Upgrade 290 Cabinet and Door Kits 291 Analytical Head Assembly (100 L) 295 Analytical-Head Assembly (900 L) 296 Analytical Head Assembly (40 L) 2972 Position/6 Port Injection Valve, 600 bar 2982 Position/6 Port Injection Valve, 800 bar 2992 Position/6 Port Injection Valve, 1300 bar 300 Agilent InfinityLab LC Series Vialsamplers User Manual8 10 Identifying Cables 301 Cable Overview 302 Analog Cables 304 Remote Cables 306 CAN/LAN Cables 310RS-232 Cables 311 USB 31211 Hardware Information 313 Firmware Description 314 Electrical Connections 317 Interfaces 319 Setting the 6-bit Configuration Switch 326 Instrument Layout 330 Early Maintenance Feedback (EMF)

10 33112 LAN Configuration 332 What You Have to Do First 333 TCP/IP parameter configuration 334 Configuration Switches 335 Initialization Mode Selection 336 Dynamic Host Configuration Protocol (DHCP) 338 Manual Configuration 341PC and Agilent ChemStation Setup 34513 Appendix 354 General Safety Information 355 Waste Electrical and Electronic Equipment (WEEE) Directive 361 Refrigerant 362 Radio Interference 365 Sound Emission 366 Solvent Information 367 Agilent Technologies on Internet 368 Agilent InfinityLab LC Series Vialsamplers User Manual91 IntroductionProduct Description (G7129A) 10 Features (G7129A) 11 Product Description (G7129B) 12 Features (G7129B) 13 Product Description (G7129C) 14 Features (G7129C) 15 Overview of the Mo