Diode Array Detector WR and Multiple Wavelength ... - Agilent

1 Diode Array Detector WR and Multiple Wavelength Detector Agilent infinitylab LC SeriesUser ManualAgilent infinitylab LC series DAD WR and MWD User ManualAgilent infinitylab LC series DAD WR and MWD User ManualNoticesDocument InformationDocument No: SD-29000218 Rev. D Part No: G7115-90000 Rev. D EDITION 02/2020 Copyright Agilent Technologies, Inc. 2016 -2020No part of this manual may be repro-duced in any form or by any means (including electronic storage and retrieval or translation into a foreign language) without prior agreement and written con-sent from Agilent Technologies, Inc.

2 As governed by United States and interna-tional copyright Technologies Hewlett-Packard-Strasse 8 76337 WaldbronnWarrantyThe material contained in this document is provided as is, and is subject to being changed, without notice, in future edi-tions. Further, to the maximum extent permitted by applicable law, Agilent dis-claims all warranties, either express or implied, with regard to this manual and any information contained herein, includ-ing but not limited to the implied warran-ties of merchantability and fitness for a particular purpose. Agilent shall not be lia-ble for errors or for incidental or conse-quential damages in connection with the furnishing, use, or performance of this document or of any information con-tained herein.

3 Should Agilent and the user have a separate written agreement with warranty terms covering the material in this document that conflict with these terms, the warranty terms in the separate agreement shall Licenses The hardware and/or software described in this document are furnished under a license and may be used or copied only in accordance with the terms of such Rights Government Restricted Rights. Soft-ware and technical data rights granted to the federal government include only those rights customarily provided to end user customers. Agilent provides this customary commercial license in Soft-ware and technical data pursuant to FAR (Technical Data) and (Computer Software) and, for the Depart-ment of Defense, DFARS (Technical Data - Commercial Items) and DFARS (Rights in Commer-cial Computer Software or Computer Software Documentation).

4 Safety NoticesCAUTIONA CAUTION notice denotes a hazard. It calls attention to an operating procedure, practice, or the like that, if not correctly per-formed or adhered to, could result in damage to the product or loss of important data. Do not proceed beyond a CAUTION notice until the indicated conditions are fully understood and met. WARNINGA WARNING notice denotes a hazard. It calls attention to an operating procedure, practice, or the like that, if not correctly per-formed or adhered to, could result in personal injury or death. Do not proceed beyond a WARN-ING notice until the indicated conditions are fully understood and infinitylab LC series DAD WR and MWD User Manual3 In This manual covers the Agilent 1260 infinity ii Diode Array Detector WR and the Agilent 1260 infinity ii Multiple Wavelength Detector modules.

5 G7115A - 1260 infinity ii DAD WR G7165A - 1260 infinity ii MWD1 Introduction This chapter gives an introduction to the Requirements and Specifications This chapter provides information on environmental requirements, physical and performance the Module This chapter explains the essential operational parameters of the the Detector This chapter provides information on how to set up the module for an analysis and explains the basic the Detector This chapter provides information on how to optimize the and Diagnostics This chapter gives an overview about the troubleshooting and diagnostic Information This chapter describes the meaning of error messages.

6 And provides information on probable causes and suggested actions how to recover from error infinitylab LC series DAD WR and MWD User Manual4 8 Test Functions and Calibration This chapter describes the tests for the This chapter describes the maintenance of the for Maintenance This chapter provides information on parts for maintenance and Cables This chapter provides information on cables used with the Agilent 1200 infinity series Information This chapter describes the Detector in more detail on hardware and Configuration This chapter provides information on connecting the module to the Agilent ChemStation This chapter provides addition information on safety.

7 Legal and infinitylab LC series DAD WR and MWD User Manual5 Contents1 Introduction 9 Introduction to the Detector 10G7115A Diode Array Detector WR 11G7165A Multiple Wavelength Detector 13 Optical System 15 Leak and Waste Handling 17 Bio-inert Materials 222 Site Requirements and Specifications 24 Site Requirements 25 Physical Specifications 28 Performance Specifications 293 Using the Module 36 Magnets 37 Turn on/off 38 Status Indicators 40 Instrument Configuration 41 Set up the Detector with Agilent Open Lab ChemStation 42 The Detector User Interface 43 Detector Control Settings 45 Method Parameter Settings 46 Agilent Local Control Modules 504 Preparing the Detector 52 Leak and Waste Handling 53 Setting up an Analysis 55 Solvent Information 62 Agilent infinitylab LC series DAD WR and MWD User Manual6 5 Optimizing the Detector 67 Optimizing the Detector Performance 68 Optimization Overview 69 Optimizing for Sensitivity, Selectivity.

8 Linearity and Dispersion 71 Optimizing Selectivity 81 Optimizing the Detector Regarding to the System 83 Warm up of the Detector 896 Troubleshooting and Diagnostics 91 Available Tests vs User Interfaces 92 Agilent Lab Advisor Software 93 Available Diagnostic Functions vs. Product Level 947 Error Information 97 What Are Error Messages 98 General Error Messages 99 Detector Error Messages 1078 Test Functions and Calibration 115 Introduction 116 Conditions of Detector 120 Failing a Test 121 Self-Test 122 Intensity Test 124 Cell Test 127 Filter Test 129 Holmium Oxide Test 131 ASTM Drift and Noise Test 134 Slit Test 138 Wavelength Verification Test 141 Wavelength Calibration 143D/A Converter (DAC)

9 Test 146 Dark-Current Test 148 Spectral Scan 150 Other Lab Advisor Functions 151 Agilent infinitylab LC series DAD WR and MWD User Manual7 9 Maintenance 152 Introduction to Maintenance 153 Cautions and Warnings 154 Overview of Maintenance 156 Cleaning the Module 157 Remove and Install Doors 158 Replace a Lamp 160 Remove and Install a Flow Cell 163 Maintenance of Standard, Semi-Micro or Micro Flow Cell 167 Maintenance of High Pressure Flow Cell 170 Replacing Capillaries on a Standard Flow Cell 172 Replacing Capillaries on a Semi-Micro and Micro Flow Cell 177 Nano Flow Cell - Replacing or Cleaning 181 Cleaning or Exchanging the Holmium Oxide Filter 185 Correcting Leaks 188 Replacing Leak Handling System Parts 190 Replacing the Module s Firmware 192 Information from Module s Assemblies 19410 Parts for Maintenance 195 Overview of Maintenance Parts 196 Standard Flow Cell 198 Standard

10 Flow Cell Bio-inert 200 Semi-Micro Flow Cell 202 Micro Flow Cell 204 High Pressure Flow Cell 206 Prep Flow Cell - SST 208 Prep Flow Cell - Quartz 210 Nano Flow Cells 212 Accessory Kits 215 Holmium Oxide Filter 216 Leak Handling Parts 217 Agilent infinitylab LC series DAD WR and MWD User Manual8 11 Identifying Cables 218 Cable Overview 219 Analog Cables 221 Remote Cables 223 BCD Cables 226 CAN/LAN Cables 228 Agilent 1200 module to PC 22912 Hardware Information 230 Firmware Description 231 Electrical Connections 234 Interfaces 236 Setting the 6-bit Configuration Switch 243 Instrument Layout 247 Early Maintenance Feedback (EMF) 24813 LAN Configuration 250 What You Have to Do First 251 TCP/IP parameter configuration 252 Configuration Switches 253 Initialization Mode Selection 254 Dynamic Host Configuration Protocol (DHCP) 256 Manual Configuration 25914 Appendix 264 General Safety Information 265 Waste Electrical and Electronic Equipment (WEEE)