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recorded with a tapping mode in air using Multimode 8 atomic force microscope (VEECO, USA). X-ray diffraction (XRD) pattern was characterized on D8 advance X-ray powder diffractometer (Bruker, Germany). Raman measurement was obtained by confocal Raman 35 microscope (CRM200, WITec) with 50× objective using excitation laser line of 532 nm.
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