Hardware / Software Installation - Agilent

1 Agilent Technologies 7820 MSD (5975 Series MSD) G7020A, G7021A Hardware and Software Installation Checklist Issued: April 20101 LSCA-GCMS Product Support 7820 MSD- Installation Page 1 of 5 Hardware / Software Installation Purpose: To ensure that instruments and systems are correctly installed and functioning as designed, in the customer's facility. Correct Installation is the first step in ensuring that instruments and systems operate reliably over an extended lifetime. Note: The 7820 MSD Diffusion pump will refer to the G3175A which is used in G7020A.

2 The 7820 MSD Standard Turbo pump will refer to the G3176A which is used in G7021A. Customer Responsibilities The customer should ensure that the Installation site is prepared in accordance with the specifications contained in the relevant site preparation document and that the necessary operating supplies, consumables and usage dependent items such as gases, vials, paper, solvents, etc. are available. A customer representative should be present at all times during the Installation . Note: During Software Installation the Support Provider will create an administrator account on the system for future use; without this capability, updating and editing of the MSD configuration files will not be possible.

3 Note: Typical Installation / familiarization times: Description Installation Familiarization 7820 AMSD hours hours G1701EA hours hours 7820A included in Bundle hours listed above Installation Checklist Unpacking and inspection of shipped materials Note: Shipping containers should not be opened until an Agilent Technologies representative is present Unpack all boxes and place equipment on bench. To prevent injury, get lifting assistance for the GC. Retain shipping containers and material until Installation is complete and performance is verified.

4 Notify order fulfillment of any discrepancies MSD ChemStation Installation Upgrade ChemStation versus new ChemStation The MSD Productivity Software will by default save/install the Software on new systems to the x:\MSDChem directory. Data System Installation and preparation (Data System needs to be configured to run Remote7820 GC panel.) Install PC with Network card Unpack LAN SWITCH and position on bench, connect the power line to the SWITCH Connect LAN cable from the GC to LAN SWITCH Port #1 Connect LAN cable from 5975 to LAN SWITCH Port #2 Agilent Technologies 7820 MSD (5975 Series MSD) G7020A, G7021A Hardware and Software Installation Checklist Issued.

5 April 20101 LSCA-GCMS Product Support 7820 MSD- Installation Page 2 of 5 Connect LAN cable from PC (T-10) to LAN SWITCH Port #3 Install printer and connect parallel cable Turn on LAN SWITCH, Modem, printer, monitor, and PC (in this order) Configure PC network for TCP/IP, IP address, Subnet Mask, as specified in the ChemStation Installation Manual. Recording Software Registration Number The Software registration number is automatically saved in the revision history file. This text file can be viewed by selecting View Revision History found in the Help menu of Data Analysis.

6 Install Agilent BOOTP Service Software (if applicable) o Turn off the MSD and GC o Turn on the MSD o Configure the MS IP address (configure BOOTP and verify communication) o Turn on GC o Configure GC IP address (configure BOOTP and verify communication) Install SICL I/O Libraries Configure the SICL I/O Libraries for LAN Client Install MSD ChemStation Productivity Software Configure the MSD and GC using MS Config icon Install MSD Service Pack (if applicable) Install Lab Monitoring and Diagnostics (LMD) Software o Manuals for the system o 7820A firmware updates o 7820A Remote Control Software Turn on both MSD and GC Using Help from the Config Icon, execute check networking and update MSD firmware.

7 Productivity Software Update Start MSD ChemStation Software by clicking instrument icon Load , verify method resolution and save to: ..1\methods\ ReLoad , a prompt for MSD Method Upgrade Detector Voltage Setting will appear. Accept the default setting and save method. Set factory tune and temperature parameters in Edit MS Params panel to (Tune and Vacuum Control) Verify profile scan is successful Save tune parameters Perform an on the system. (This will perform the traditional ATUNE as well as update the GAIN profile for the tune.)

8 Update and save other evaluation methods (if applicable) ..\1\5975\ Validate the methods are still GAIN based methods, by reloading them after saving .. Gain setting 15 .. Gain setting 1 Agilent Technologies 7820 MSD (5975 Series MSD) G7020A, G7021A Hardware and Software Installation Checklist Issued: April 20101 LSCA-GCMS Product Support 7820 MSD- Installation Page 3 of 5 GC Installation and preparation if applicable. Remove left side panel of GC Remove upper front knockout in the GC exterior oven wall for MSD interface Remove the two knockouts from the left side panel.

9 Disconnect the rear inlet heater/sensor cable for the MSD interface o If rear inlet has an inlet then connect GC auxiliary heating cable Reinstall left side panel, route GC/MSD interface cable through the lower hole Connect carrier gas, trap, and GC with copper tubing Purge gas lines with helium at 5 - 8 psi (35 - 55 KPa) Install ALS (optional) Verify line voltage and outlet Plug in power cable and turn on GC Verify that the GC passes self test Configure Column parameters using Software keyboard Set carrier gas line pressure to approximately 50 psi (448 KPa)

10 Set carrier gas flow rate to 3 ml per minute Remove septum plugging end of column and cut end of column Verify helium flow through column Set Injection port temperature to 300 C Set oven temperature to ramp from 40 C to 280 C at 15 C per minute, and hold for 10 minutes. Inject a solvent sample into GC; repeat two more times, 5 minutes apart Set GC temperature to 40 C after temperature cycle complete MSD Installation and preparation Unpack MSD Unpack Foreline pump and add oil to pump Unpack Foreline pump safety cage (optional) Place MSD and foreline pump on the bench Open the top cover of MSD Fill the PFTBA calibrant vial with calibrant (if applicable)